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• 1D ³¹P without ¹H decoupling experiment.
• Quantitative 1D ¹³C experiment.

• Estimating molecular weights with DOSY
• 2D ¹H-²⁹Si HMBC experiment

• DEPTQ
• Solid State HETCOR
•  More on Pure shift ¹H NMR: PSYCHE.

•  ¹⁹F NMR Spectroscopy
•  1D ¹H Quantitative NMR
•  2D-J Resolved ¹H NMR Spectroscopy

•   2D-J Resolved ¹H NMR Spectroscopy
•  Pure shift ¹H NMR

•  12 minutes that can save you a lot of time!!
•  Cross Polarization Magic Angle Spinning (CPMAS).CPMAS  versus  VACPMAS.

•  ¹⁴Nitrogen J coupling.
•  ²⁹Si Satellite lines

• ¹⁵N HMBC experiment.

•  Diffusion-Ordered Spectroscopy (DOSY)

•  Integration of ¹H NMR lines. Quantitative NMR

• Dr. E. Serpersu research work. Dept. of Biochemistry & Cellular and Molecular Biology.
  JACS 131,8587-8594 (2009)

•  Measuring dihedral angles by NMR
•  Determination of Inter-glycosidic Coupling Constants from
•  J-modulated HMBC spectra

•   NMR in Forensic Science

•  What is the structure of the molecule I have sensitized? Is it trans or cis?

• NMR-Related Research in Dr. B. Xue’s  Group

•  HSQC or ¹³C spectrum, which one has the highest sensitivity?
•  How hard is to run 2D experiments?
•  Do you want to save time? …then run 2D experiments!
•  The fastest 2D experiment:  COSY (it takes only 3minutes!).

•  Do you want to save time? …then run 2D experiments!

•   Measuring Residual Dipolar Couplings (RDCs)